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Ultraperformance liquid chromatography–mass spectrometry (UPLC-MS) analysis of Kratom extracts Untargeted metabolomics analyses were conducted using an Acquity Ultra-Performance Liquid Chromatography system (Waters, Milford, MA, USA) coupled to a Q Exactive Plus Hybrid Quadrupole-Orbitrap mass spectrometer (Thermo Fisher Scientific, Waltham, MA)